Background: Often, claims in Component-Based Development (CBD) are only sup-
ported by qualitative expert opinion, rather than by quantitative data. This contrasts
with the normal practice in other sciences, where a sound experimental validation of
claims is standard practice. Experimental Software Engineering (ESE) aims to bridge
this gap. Unfortunately, it is common to find experimental validation efforts that are
hard to replicate and compare, to build up the body of knowledge in CBD.

Objectives: In this dissertation our goals are (i) to contribute to evolution of ESE, in
what concerns the replicability and comparability of experimental work, and (ii) to ap-
ply our proposals to CBD, thus contributing to its deeper and sounder understanding.

Techniques: We propose a process model for ESE, aligned with current experimen-
tal best practices, and combine this model with a measurement technique called
Ontology-Driven Measurement (ODM). ODM is aimed at improving the state of prac-
tice in metrics definition and collection, by making metrics definitions formal and ex-
ecutable, without sacrificing their usability. ODM uses standard technologies that can
be well adapted to current integrated development environments.

Results: Our contributions include the definition and preliminary validation of a pro-
cess model for ESE and the proposal of ODM for supporting metrics definition and
collection in the context of CBD. We use both the process model and ODM to perform
a series experimental works in CBD, including the cross-validation of a component
metrics set for JavaBeans, a case study on the influence of practitioners expertise in
a sub-process of component development (component code inspections), and an ob-
servational study on reusability patterns of pluggable components (Eclipse plug-ins).
These experimental works implied proposing, adapting, or selecting adequate ontolo-
gies, as well as the formal definition of metrics upon each of those ontologies.

Limitations: Although our experimental work covers a variety of component models
and, orthogonally, both process and product, the plethora of opportunities for using
our quantitative approach to CBD is far from exhausted.

Conclusions: The main contribution of this dissertation is the illustration, through
practical examples, of how we can combine our experimental process model with
ODM to support the experimental validation of claims in the context of CBD, in a re-
peatable and comparableway. In addition, the techniques proposed in this dissertation
are generic and can be applied to other software development paradigms.

Software transactional memory (STM) is a promising programming model that adapts many concepts borrowed from the databases world to control concurrent accesses to memory (RAM) locations. In this paper we propose a new classification for the active states of a transaction; a new memory quiescing algorithm, to allow the safe transition of a memory block form transactional to non-transactional space; we compare word and object transactional grain units; and evaluate the cost of consistent state validation, arguing that this cost can be minimized by performing partial validation on problematic code regions.

n/a

n/a

n/a

n/a

The characterization of the bottom ashes produced by two Portuguese municipal solid waste incinerators (MSWI) was performed with the aim of assessing the feasibility of using this waste as raw material in the production of glass that can be further processed as glass-ceramics for application in construction. Density and particle size distribution measurements were carried out for physical characterization. Chemical characterization revealed that SiO2, a network glass former oxide, was present in a relatively high content (52-58 wt%), indicating the suitability for this waste to be employed in the development of vitreous materials. CaO, Na2O and K2O, which act as fluxing agents, were present in various amounts (2-17 wt%) together with several other oxides normally present in ceramic and glass raw materials. Mineralogical characterization revealed that the main crystalline phases were quartz (SiO2) and calcite (CaCO3) and that minor amounts of different alkaline and alkaline-earth aluminosilicate phases were also present. Thermal characterization showed that the decomposition of the different compounds occurred up to 1100 °C and that total weight loss was <10 wt%. Heating both bottom ashes at 1400 °C for 2 h resulted in a melt with suitable viscosity to be poured into a mould, and homogeneous black-coloured glasses with a smooth shiny surface were obtained after cooling. The vitrified bottom ashes were totally amorphous as confirmed by X-ray diffraction. The results from the present experimental work indicate that the examined bottom ashes can be a potential material to melt and to obtain a glass that can be further processed as glass-ceramics to be applied in construction. © 2007 Elsevier Ltd. All rights reserved.

n/a

Nanotechnology is having a positive impact on nearly every industry, and in particular in healthcare, where it is extending the limits of molecular diagnostics to the nanoscale-nanodiagnostics. Here we describe an innovative optoelectronic platform for the colorimetric detection of nucleic acids based on oligonucleotide-derivatized gold nanoparticles. The device integrates an amorphous/nanocrystalline biosensor and a light emission source with a gold nanoprobe for specific DNA detection. This low cost, fast and simple optoelectronic platform permits detection of few picomole of nucleic acid without target or signal amplification making it suitable for application in population diagnostics and in point-of-care hand-held devices. © 2007 Elsevier B.V. All rights reserved.

n/a

n/a

This paper presents an analytical model for CMOS delay and power estimation in deep sub micrometer technologies. In this paper the EKV transistor model is considered as a way of granting the accuracy of results in the characterization of deep submicron CMOS circuits. The analytical model proposed is valid for a ramp input signal, and takes into account all the operation regions of the transistor as well the influence of the gate-to-drain capacitance. For estimating the power consumption, a simple numerical integration process is applied to the current wave. An application example considering the use of the model for the evaluation of the delay and power consumption associated to a CMOS inverter is considered. The validity of the results obtained with the proposed model for a 1.2V TSMCN65 CMOS inverter is checked against those obtained through Hspice simulation.

N, (N+Ga) and (N+Al) doped ZnO films were deposited on c-plane sapphire substrates by RF magnetron sputtering at room temperature. The samples were characterized by their structural, surface morphological, compositional and optical properties. The x-ray diffraction studies confirmed the co-doping of (N+Ga) and (N+Al) besides showing improvement in the crystallinity when compared with the single Ndoping. The surface of the films becomes rougher after co-doping. The x-ray photoelectron spectroscopy and Rutherford back-scattering analysis indicate that the co-doping changes the chemical states and varies the amount of nitrogen (N) in ZnO. The amount of 'N' has been greatly increased for (N+Ga) co-doping, indicating that it is the best co-doping pair for p-type ZnO. Additionally, co-doping has increased the average visible transmittance (40-650nm) and the optical band gap is shifted towards shorter wavelength. In the case of (N+Al) co-doping, the band gap becomes wider than that of undoped ZnO. © IOP Publishing Ltd.

n/a

In this work we studied indium zinc oxide (IZO) thin films deposited by r.f. magnetron sputtering at room temperature. The films were annealed at high temperature (1100 K) in vacuum, and the oxygen exodiffusion was monitored in-situ. The results showed three main peaks, one at approximately 600 K, other at approximately 850 K and the last one at 940 K, which are probably from oxygen bonded in the film surface and in the bulk, respectively. The initial amorphous structure becomes microcrystalline, according to the X-ray diffraction. The electrical conductivity of the films decreases (about 3 orders of magnitude), after the annealing treatment. This behavior could be explained by the crystallization of the structure, which affects the transport mechanism. Apart from the changes in the material structure, a small variation was observed on the absorption coefficient. © 2007 Elsevier B.V. All rights reserved.

n/a

Sulphate-reducing bacteria have a wide variety of periplasmic cytochromes involved in electron transfer from the periplasm to the cytoplasm. HmcA is a high molecular mass cytochrome of 550 amino acid residues that harbours 16 c-type heme groups. We report the crystal structure of HmcA isolated from the periplasm of Desulfovibrio gigas. Crystals were grown. using polyethylene glycol 8K and zinc acetate, and diffracted beyond 2.1 angstrom resolution. A multiple-wavelength anomalous dispersion experiment at the iron absorption edge enabled us to obtain good-quality phases for structure solution and model building. DgHmcA has a V-shape architecture, already observed in HmcA isolated from Desulfovibrio vulgaris Hildenborough. The presence of an oligosaccharide molecule covalently bound to an Asn residue was observed in the electron density maps of DgHmcA and confirmed by mass spectrometry. Three modified monosaccharides appear at the highly hydrophobic vertex, possibly acting as an anchor of the protein to the cytoplasmic membrane. (c) 2007 Elsevier Ltd. All rights reserved.

The electric and magnetic properties of high temperature superconductors and the possibility to cool them by cheap liquid nitrogen makes them attractive in power applications. An all superconducting linear synchronous motor is presented in this paper in order to quantify the benefits and disadvantages of such applications. The term ?all superconducting? is related with the absence of copper conductors and iron parts. Certain characteristics of the superconducting materials impose severe restrictions when used, e.g., as armature windings. A numerical method for deriving the thrust and lift forces developed in such a motor, driven by a typical current inverter, is presented.

n/a

n/a

Most of the discussion and controversy on organisation of work concepts has been referenced to the manufacturing industry along the 20th century: it started with the concept of “scientific management” from Taylor, and continued with the new ideas on the importance of human factors as Mayo pointed out in the 1930s. Immediately after the 2nd World War Friedmann studied the human problems related to new manufacturing technologies and automation. And the late 1950 and 1960s were decades of strong debate on the socio-technics with the research at Tavistock Institute of London and the emergence of national programmes on new forms of work organisation. At the end of the last century the concept of collaborative work was developed together with the definition(s) of information systems and organisational design. However, the interest came from other production activities, like the services. This article analyses the approaches developed on these debates on the collaborative work and information system and its application to the manufacturing industry.

n/a

In 1999, the DEECA/INETI and the UBiA/FCT/UNL started a researching project on the partition of heavy metals during the combustion of stabilised sewage sludge (Biogran®), in a fluidised-bed reactor, and on the quality of the bottom ashes and fly ashes produced. This project was entitled Bimetal and was funded by the Portuguese Foundation for Science and Technology. In this paper only the results on the combustion of Biogran® are reported. The combustion process was performed in two different trials, in which different amounts of sewage sludge and time of combustion were applied. Several ash samples were collected from the bed (bottom ashes) and from two cyclones (first cyclone and second cyclone ashes). Sewage sludge, bed material (sand) and ash samples were submitted to the leaching process defined in the European leaching standard EN 12457-2. The eluates were characterized for a set of inorganic chemical species. The ecotoxicological levels of the eluates were determined for two biological indicators (Vibrio fischeri and Daphnia magna). The results were compared with the limit values of the CEMWE French Regulation. The samples were also ranked according to an index based on the chemical characterization of the eluates. It was observed an increase of the concentration of metals along the combustion system. The ashes trapped in the second cyclone, for both combustion trials, showed the highest concentration of metals in the eluates. Chemically, the ashes of the second cyclone were the most different ones. In the ecotoxicological point of view, the ecotoxicity levels of the eluates of the ashes, for both combustion cycles, did not follow the same pattern as observed for the chemical characterization. The ashes of the first cyclone showed the highest ecotoxicity levels for V. fischeri and D. magna. This difference on chemical and ecotoxicological results proves the need for performing both chemical and ecotoxicological characterizations of the sub-products of such type of thermal processes.