Abstract This work addresses the experimental identification of mode I cohesive law of wood bonded joints. The approach combines the double cantilever beam (DCB) test with both digital image correlation (DIC) and embedded fibre Bragg grating (FBG) sensors. The spectrum geometric mean of the \{FBG\} reflected spectral response was determined, and the wavelength evolution was used to define the fracture process zone (FPZ) development phase. This evaluation allowed a consistent selection of experimental range of over which the identification procedure of mode I cohesive law is build up. Mode I crack length, Resistance-curve and cohesive law parameters are characterised and discussed. The strain energy release rate (GI) is determined from the P�d curve by the compliance-based beam method (CBBM). The crack tip opening displacement (wI) is determined by post-processing displacements measured by DIC. The cohesive law in mode I (sI�wI) is then obtained by numerical differentiation of the GI�wI relationship.

Abstract Several analyses of diversity through geological time use global, synoptic databases, and this practice often makes it difficult to distinguish true signals in changing diversity from regional-scale sampling and/or geological artefacts. Here we investigate how echinoid diversity changed through the Mesozoic of the Lusitanian basin in Portugal based on a comprehensive, revised database, and seek to distinguish biological signal from geological or environmental constraints. The observed diversity pattern is far from having a defined trend, showing many fluctuations that appear to be linked with gaps in the geological record. This study revealed that, independently of the method used, whether correlation tests or model fitting, the diversity signal is not completely explained by the studied sampling proxies. Among the different proxies, marine facies variation in combination with outcrop area best explains the palaeodiversity curve.

Supply Chain Design problems often result into multiperiod stochastic mixed integer problems that are hard to solve. In this paper we propose a metaheuristic algorithm as a specialization for two- stage problems of the so-named Fix-and-Relax Algorithm presented previously for solving large- scale multiperiod stochastic mixed 0-1 optimization problems under a time stochastic dominance risk averse strategy, so-named TSD. Some computational experience is presented.

Goal-oriented Requirements Engineering approaches have become popular in the Requirements Engineering community as they provide expressive modelling languages for requirements elicitation and analysis. However, as a common challenge, such approaches are still struggling when it comes to managing the accidental complexity of their models. Furthermore, those models might be incomplete, resulting in insufficient information for proper understanding and implementation. In this paper, we provide a set of metrics, which are formally specified and have tool support, to measure and analyse complexity and completeness of goal models, in particular social goal models (e.g. i⁎). Concerning complexity, the aim is to identify refactoring opportunities to improve the modularity of those models, and consequently reduce their accidental complexity. With respect to completeness, the goal is to automatically detect model incompleteness. We evaluate these metrics by applying them to a set of well-known system models from industry and academia. Our results suggest refactoring opportunities in the evaluated models, and provide a timely feedback mechanism for requirements engineers on how close they are to completing their models.

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http://docentes.fct.unl.pt/lblm/files/jbic-2015-20-181.pdf

http://docentes.fct.unl.pt/lblm/files/jbic-2015-20-287.pdf

Let $G$ be a graph whose edges are coloured with $k$ colours, and $\mathcal H=(H_1,\dots , H_k)$ be a $k$-tuple of graphs. A \emph{monochromatic $\mathcal H$-decomposition} of $G$ is a partition of the edge set of $G$ such that each part is either a single edge or forms a monochromatic copy of $H_i$ in colour $i$, for some $1\le i\le k$. Let $\phi_{k}(n,\mathcal H)$ be the smallest number $\phi$, such that, for every
order-$n$ graph and every $k$-edge-colouring, there is a monochromatic $\mathcal H$-decomposition with at most $\phi$ elements. Extending the previous results of Liu and Sousa [``Monochromatic $K_r$-decompositions of graphs", \emph{Journal of Graph Theory}76:89-100,2014], we solve this problem
when each graph in $\mathcal H$ is a clique and $n\ge n_0(\mathcal H)$ is sufficiently large.

A tecnologia e o impacto que esta pode ter sobre as diferentes representações utilizadas e, em particular, sobre a representação algébrica são o foco deste artigo. Procura-se assim compreender como é que o professor enquadra a representação algébrica no trabalho em sala de aula e como a procura tornar relevante para os alunos num contexto de utilização da tecnologia. As conclusões alcançadas apontam para a opção por uma estreita articulação entre as representações algébrica e gráfica e para uma criteriosa escolha de tarefas, envolvendo múltiplas abordagens, onde a representação algébrica vem disponibilizar informação fundamental e tendencialmente inacessível a partir de outras representações.

Transparent metal oxides thin films are a class of inorganic conductors and semiconductors with significant importance for use in portable electronics, displays, flexible electronics, multi-functional windows and solar cells. Due to the recent development of transparent and flexible electronics, there is a growing interest in depositing metal-oxide thin-film on plastic substrates that can offer flexibility, lighter weight, and potentially lead to cheaper manufacturing by allowing printing and rollto- roll processing. The plastic substrates, however, limit device processing to below 200oC. In this context, the deposition of high-performance semiconductor thin films from dispersions of pre-prepared oxide nanoparticles at temperatures below 200oC represents a potential key route. This paper reports on the preparation of ZnO transparent thin films using solutionprocessed nanoparticles (NPs) precipitated from zinc acetate alcoholic solution with potassium hydroxide. The nanoparticles size distribution, microstructure and crystallinity were measured by dynamic light scattering (DLS), Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD). The thin films were deposited by spin-coating onto soda lima glass substrate, using a dispersion of 1wt% ZnO NPs. The morphology of the films annealed at 120 and 180oC, observed by atomic force microscopy and cross-section scanning electron microscopy, shows columnar grains with diameter ranging between 20 and 70 nm, depending on the conditions of depositions. Optical measurements indicated high transparency, between 85 and 94 %, in the visible range, a direct nature of band-to-band transitions and band gap values between 3,22 and 3,32 eV. The refractive index and extinction coefficient have been calculated from optical transmittance and reflectance spectra.

The orange protein (ORP) isolated from the sulfate-reducing bacterium Desulfovibrio gigas (11.8 kDa) contains a mixed-metal sulfide cluster of the type [S2MoS2CuS2MoS2](3-) noncovalently bound to the polypeptide chain. The D. gigas ORP was heterologously produced in Escherichia coli in the apo form. Different strategies were used to reconstitute the metal cluster into apo-ORP and obtain insights into the metal cluster synthesis: (1) incorporation of a synthesized inorganic analogue of the native metal cluster and (2) the in situ synthesis of the metal cluster on the addition to apo-ORP of copper chloride and tetrathiomolybdate or tetrathiotungstate. This latter procedure was successful, and the visible spectrum of the Mo-Cu reconstituted ORP is identical to the one reported for the native protein with absorption maxima at 340 and 480 nm. The (1)H-(15)N heteronuclear single quantum coherence spectra of the reconstituted ORP obtained by strategy 2, in contrast to strategy 1, exhibited large changes, which required sequential assignment in order to identify, by chemical shift differences, the residues affected by the incorporation of the cluster, which is stabilized inside the protein by both electrostatic and hydrophobic interactions.

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