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Arteiro, A., G. Catalanotti, J. Xavier, P. Linde, and P. P. Camanho. "A strategy to improve the structural performance of non-crimp fabric thin-ply laminates." Composite Structures. 188 (2018): 438-449. AbstractWebsite

The enhanced mechanical performance of thin-ply laminates results from their ability to delay the onset of damage typically observed in composite materials. However, in notched structures, subcritical damage growth causes beneficial stress redistributions in the vicinity of the notch, blunting the stress concentration. Precluding these damage mechanisms, as in thin-ply laminates, may potentially lead to inferior notched responses. To obviate this limitation of thin-ply laminates, a strategy based on the combination of standard grade 0� plies and thin transverse and off-axis plies is analysed in this paper. A detailed study of the effect of 0� ply blocking is carried out, with particular emphasis on the blunting mechanisms and notched response. Tests on scaled notched panels loaded in tension, with notch sizes between 6?mm and 30?mm, show that the combination of standard grade 0� ply blocks with thin transverse and off-axis plies promotes localised fibre-matrix splitting, which acts as an important notch blunting mechanism, while preventing matrix cracking and delamination. This results in an improved notched response and superior large damage capability. It is also shown that thicker 0� ply blocks provide higher stability in composite bolted joints, while the thin transverse and off-axis plies contribute for matrix-dominated damage suppression, resulting in an improved bolt-bearing response. The improvements of the large damage capability and bolt-bearing performance are obtained without compromising the superior unnotched tensile and compressive strengths intrinsic to thin-ply laminates.

Ercin, G. H., P. P. Camanho, J. Xavier, G. Catalanotti, S. Mahdi, and P. Linde. "Size effects on the tensile and compressive failure of notched composite laminates." Composite Structures. 96 (2013): 736-744. Abstract
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Furtado, C., A. Arteiro, G. Catalanotti, J. Xavier, and P. P. Camanho. "Selective ply-level hybridisation for improved notched response of composite laminates." Composite Structures. 145 (2016): 1-14. AbstractWebsite

Abstract This work presents an experimental study on the effect of ply-level hybridisation on the tensile unnotched and notched response of composite laminates. In a first assessment, notched tests were performed on laminates with nominal ply thicknesses between 0.03 mm and 0.30 mm. From the understanding of the effect of ply thickness on the damage mechanisms that govern the notched response of laminates, the concept of ply-level hybridisation is introduced, which consists in combining plies of different grades. A uniform combination of thin and conventional plies resulted in a hybrid laminate with intermediate notched response. Selective hybridisation, where thin off-axis plies are combined with thicker 0° plies, resulted in a globally enhanced notched behaviour without compromising the unnotched and fatigue responses. This work clearly shows how ply-level hybridisation, when designed to trigger specific damage mechanisms, can be used to improve the notched response of composite laminates.

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Sampayo, L. M. C. M. V., P. M. F. Monteiro, J. A. F. O. Correia, J. M. C. Xavier, De A. M. P. Jesus, A. Fernandez-Canteli, and R. A. B. Calçada. "Probabilistic S-N Field Assessment for a Notched Plate Made of Puddle Iron From the Eiffel Bridge with an Elliptical Hole." Procedia Engineering. 114 (2015): 691-698. AbstractWebsite

Abstract Probabilistic fatigue models are required to account conveniently for several sources of uncertainty arising in the prediction procedures for structural details, such as the scatter in material behaviour. In this paper, a procedure to derive probabilistic S-N fields for structural details [1] is applied to a notched geometry with elliptic central hole made of puddle iron from the Eiffel bridge, based on the local approaches supported by the probabilistic ɛa–N or Smith–Watson–Topper (SWT)–N fields [1,2]. This procedure suggests an extension of the fatigue crack propagation model proposed by Noroozi et al. [3,4] to structural details, in order to cover both the fatigue crack initiation and fatigue crack propagation, based on local strain approaches to fatigue. Both fatigue crack initiation and fatigue crack propagation mechanisms are accounted for in the proposed approach. The numerical results are compared with available experimental S-N fatigue data for the notched plate under consideration.

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Rodrigues, M. F., J. Correia, B. Pedrosa, A. de Jesus, B. Carvalho, C. Rebelo, J. Xavier, and R. Calçada. "Numerical analysis of a double shear standard bolted connection considering monotonic loadings." Engineering Structures and Technologies. 9 (2017): 183-194. AbstractWebsite

AbstractThe behaviour of standard boltedsteel connections submitted to monotonic loads, through the use of numerical models, is presented in the current paper.The bolted connections allow speed up constructive processes in an increasingly competitive and globalized world in which the costs are a decisive factor in the development of a project. The use of computational tools in the analysis of bolted connections becomes determinant, mainly for new solutions or solutions less explored in terms of design codes.Throughout the years, bolted connections have been suffering transformations resulting from research activities performed by many authors. Rivets have been replaced by bolts, the main achievement being the pre-stressed bolts. Methodologies based on finite element analyses were proposed for double shear bolted connection. The non-linear behaviour of these connections is investigated and their performances are compared. In the numerical modelling of the bolted connection, linear elastic and elastoplastic analyzes reveal that there are two slip levels associated with local non-linearities caused by the contact pairs, which vary with clamping stresses.

Arteiro, A., C. Catalanotti, J. Xavier, and P. P. Camanho. "Notched response of non-crimp fabric thin-ply laminates: analysis methods." Composites Science and Technology. 88 (2013): 165-171. Abstract
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Arteiro, A., G. Catalanotti, J. Xavier, and P. P. Camanho. "Notched response of non-crimp fabric thin-ply laminates." Composites Science and Technology. 79 (2013): 97-114. Abstract
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Catalanotti, G., and J. Xavier. "Measurement of the mode II intralaminar fracture toughness and R-curve of polymer composites using a modified Iosipescu specimen and the size effect law." Engineering Fracture Mechanics. 138 (2015): 202-214. AbstractWebsite

Abstract A modified Iosipescu specimen is proposed to measure the mode İI\} intralaminar fracture toughness and the corresponding crack resistance curve of fibre reinforced composites. Due to the impossibility of scaling the specimen, a modification of the classical size effect method is proposed. The calculation of the crack driving force curves is performed using the Finite Element Method. The classical Iosipescu shear feature was used and tests were coupled with digital image correlation to support the proposed approach. Experiments were performed on IM7/8552 material system and the R-curve was obtained. The steady-state value of the fracture toughness of the ply is found to be equal to R 0 ss = 34.4  kJ/m2.

Catalanotti, C., J. Xavier, and P. P. Camanho. "Measurement of the compressive crack resistance curve of composites using the size effect law." Composites Part A: Applied Science and Manufacturing. 56 (2014): 300-307. Abstract
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Catalanotti, G., P. P. Camanho, J. Xavier, C. G. Dávila, and AT Marques. "Measurement of resistance curves in the longitudinal failure of composites using digital image correlation." Composites Science and Technology. 70 (2010): 1986-1993. Abstract
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Pereira, J. C. R., A. M. P. de Jesus, J. Xavier, J. A. F. O. Correia, L. Susmel, and A. A. Fernandes. "Low and ultra-low-cycle fatigue behavior of X52 piping steel based on theory of critical distances." International Journal of Fatigue (2020): 105482. AbstractWebsite

The cyclic failure observed in structural components such as pipelines subjected to extreme loading conditions highlights some limitations concerning the application of existing fatigue damage models. The evaluation and prediction of this type of failure in these steel components under large-scale plastic yielding associated with high levels of stress triaxiality are not sufficiently known nor explored. This fatigue domain is conventionally called ultra-low-cycle fatigue (ULCF) and damage features are representative of both low-cycle fatigue (LCF) and monotonic ductile fracture. Thus, in order to understand the ULCF damage mechanisms both monotonic and LCF tests are required to get representative bounding damage information to model the material damage behaviour under such extreme loading conditions. This paper aims at exploring the Theory of Critical Distances (TCD) in the LCF and ULCF fatigue regimes, including the application of the point, line and area methods. The application of the TCD theories has not been explored so far in the ULCF fatigue regimes, despite its promising results in the LCF and high-cycle fatigue. An experimental program was carried out on several specimens’ geometries made of X52 piping steel. In detail, smooth plane specimens and notched plane specimens were cyclic loaded under tension/compression loading in order to obtain fatigue lives within the range of 101-104 cycles. In addition, cyclic bending tests on notched plane specimens were also incorporated in this study. Finite element simulations of all small-scale tests were conducted allowing to derive elastoplastic stress/strain fields along the potential crack paths. The numerical data were subjected to a post-processing in order to find characteristic lengths that can be treated as a fatigue property according to the TCD. A unified strain-life relation is proposed for the X52 piping steel together with a characteristic material length, consisting of a practical relation for pipeline strain-based design under extreme cyclic loading conditions.

Arteiro, A., G. Catalanotti, J. Xavier, and P. P. Camanho. "Large damage capability of non-crimp fabric thin-ply laminates." Composites Part A: Applied Science and Manufacturing. 63 (2014): 110-122. AbstractWebsite
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Kuhn, P., H. Koerber, G. Catalanotti, and J. Xavier. "Intralaminar fracture toughness of UD glass fiber composite under high rate fiber tension and fiber compression loading." EPJ Web Conferences. 183 (2018): 02018. AbstractWebsite

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Catalanotti, G., P. Kuhn, J. Xavier, and H. Koerber. "High strain rate characterisation of intralaminar fracture toughness of GFRPs for longitudinal tension and compression failure." Composite Structures. 240 (2020): 112068. AbstractWebsite

The elastic parameters, strengths, and intralaminar fracture toughness are determined for an E-Glass polymer composite material system, statically and at high strain rate, adapting methodologies previously developed by the authors for different carbon composites. Dynamic experiments are conducted using tension and compression Split-Hopkinson Bars (SHBs). A unique set of experimental parameters is obtained, and reported together with the experimental set-up, in order to ensure reproducibility. While in-plane elastic and strength properties were obtained by testing one specimen geometry, intralaminar fracture properties required the testing of different sized notched specimens with scaled geometries. This allowed the use of the size-effect method for the determination of the dynamic R-curve. When comparing these results with those previously obtained for a carbon/epoxy material system, it is observed that the dynamic fracture toughness exhibits a much more significant increase in both tension and compression. The obtained results permit the identification of the softening law at different strain rates, allowing its use in any analytical or numerical strength predictive method.

Koerber, H., J. Xavier, P. P. Camanho, Y. E. Essa, and Martín F. de la Escalera. "High strain rate behaviour of 5-harness-satin weave fabric carbon–epoxy composite under compression and combined compression–shear loading." International Journal of Solids and Structures. 54 (2015): 172-182. AbstractWebsite

Abstract The strain rate dependent mechanical behaviour was studied for the common out-of-autoclave aerospace textile composite 5-harness-satin carbon–epoxy. End-loaded 15 ° , 30 ° and 45 ° off-axis and 90 ° compression tests were carried out at three different strain rate levels ( 4 × 10 - 4 s - 1 , 200 s - 1 and 1000 s - 1 ) to determine the effect of strain rate for transverse compression and combined transverse compression/in-plane shear loading. The dynamic tests were carried out on a split-Hopkinson pressure bar, where high speed photography and digital image correlation allowed a detailed study of the specimen deformation and failure process. Quasi-static reference tests were carried out on an electro-mechanical test machine using the same specimen type and a static \{DIC\} system. Pronounced strain rate effects on the axial stress–strain response were observed for all specimen types. Failure envelopes for the combined σ 22 c - τ 12 stress state were derived from the experimental data and compared with the maximum stress criterion, which appears well suited to approximate the experimental failure envelope at all strain rate levels. It was observed that the failure envelope was simply scaled up with increasing strain rate, while the overall shape was found to be strain rate independent.

Koerber, H., J. Xavier, P. P. Camanho, Y. E. Essa, and Martín F. de la Escalera. "High strain rate behaviour of 5-harness-satin weave fabric carbon-epoxy composite under compression and combined compression-shear loading." International Journal of Solids and Structures. 54 (2015): 172-182. AbstractWebsite

Abstract The strain rate dependent mechanical behaviour was studied for the common out-of-autoclave aerospace textile composite 5-harness-satin carbon�epoxy. End-loaded 15 � , 30 � and 45 � off-axis and 90 � compression tests were carried out at three different strain rate levels ( 4 � 10 - 4 s - 1 , 200 s - 1 and 1000 s - 1 ) to determine the effect of strain rate for transverse compression and combined transverse compression/in-plane shear loading. The dynamic tests were carried out on a split-Hopkinson pressure bar, where high speed photography and digital image correlation allowed a detailed study of the specimen deformation and failure process. Quasi-static reference tests were carried out on an electro-mechanical test machine using the same specimen type and a static \{DIC\} system. Pronounced strain rate effects on the axial stress�strain response were observed for all specimen types. Failure envelopes for the combined s 22 c - t 12 stress state were derived from the experimental data and compared with the maximum stress criterion, which appears well suited to approximate the experimental failure envelope at all strain rate levels. It was observed that the failure envelope was simply scaled up with increasing strain rate, while the overall shape was found to be strain rate independent.

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Kuhn, P., G. Catalanotti, J. Xavier, P. P. Camanho, and H. Koerber. "Fracture toughness and crack resistance curves for fiber compressive failure mode in polymer composites under high rate loading." Composite Structures. 182 (2017): 164-175. AbstractWebsite

Abstract This work presents an experimental method to measure the compressive crack resistance curve of fiber-reinforced polymer composites when subjected to dynamic loading. The data reduction couples the concepts of energy release rate, size effect law and R-curve. Double-edge notched specimens of four different sizes are used. Both split-Hopkinson pressure bar and quasi-static reference tests are performed. The full crack resistance curves at both investigated strain rate regimes are obtained on the basis of quasi-static fracture analysis theory. The results show that the steady state fracture toughness of the fiber compressive failure mode of the unidirectional carbon-epoxy composite material IM7-8552 is 165.6kJ/m2 and 101.6kJ/m2 under dynamic and quasi-static loading, respectively. Therefore the intralaminar fracture toughness in compression is found to increase with increasing strain rate.

Arteiro, A., G. Catalanotti, J. Xavier, and P. P. Camanho. "A Finite Fracture Mechanics Model for the Prediction of the Notched Response and Large Damage Capability of Composite Laminates." Advances in Fracture and Damage Mechanics XIII. Vol. 627. Key Engineering Materials, 627. Trans Tech Publications, 2015. 13-16. Abstract

A new model based on Finite Fracture Mechanics (FFMs) has been proposed to predict the open-hole tensile strength of composite laminates [1]. Failure is predicted when bothstress-based and energy-based criteria are satisfied. This model is based on an analytical solution, and no empirical adjusting parameters are required, but only two material properties: the unnotched strength and the fracture toughness. In the present work, an extension of the proposed FFMs model to predict the notched response of composite laminates with notch geometries other than a circular opening [2] is presented and applied to the prediction of size effects on the tensile and compressive notched strength of composite laminates. The present model is also used to assess the notch sensitivity and brittleness of composite laminates by means of versatile design charts and by the identification of a dimensionless parameter designated as notch sensitivity factor. A further extension of the FFMs model is proposed, which takes into account the crack resistance curve of the laminate in the model's formulation, and it is used to predict the large damage capability of a non-crimp fabric thin-ply laminate [3].

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Silva, Patrícia, Pedro Fernandes, José Sena-Cruz, José Xavier, Fernando Castro, Delfim Soares, and Vítor Carneiro. "Effects of different environmental conditions on the mechanical characteristics of a structural epoxy." Composites Part B: Engineering. 88 (2016): 55-63. AbstractWebsite

Abstract With the aim of characterising a commercially available epoxy adhesive used for fibre-reinforced polymers strengthening applications, when submitted to different environmental conditions, mainly thermal (TC), freeze–thaw (FT), and wet–dry (WD) cycles and immersion in pure (PW) and water with chlorides (CW) for periods of exposure that lasted up to 16 months, an experimental program was carried out. Several methodologies were used in its characterization, mainly the scanning electron microscope (SEM), dynamic mechanical analysis (DMA), standard tensile tests (STT) coupled with digital image correlation (DIC). In general the results revealed that the chemical composition was not affected by the environmental conditions. Nevertheless, it was verified through \{DMA\} and \{STT\} that the modulus of elasticity and tensile strength of the epoxy adhesive increased in the TC, while the specimens submitted to \{PW\} and \{CW\} faced a high degradation in terms of its mechanical properties. Eventually, the glass transition temperature (Tg) was not affected by the environmental conditions, apart from the specimens subjected to \{TC\} and FT, presenting a higher and lower Tg, respectively, when compared with the reference specimens.

Arteiro, A., G. Catalanotti, J. Xavier, P. Linde, and P. P. Camanho. "Effect of tow thickness on the structural response of aerospace-grade spread-tow fabrics." Composite Structures. 179 (2017): 208-223. AbstractWebsite

The effect of ply thickness on the onset of intralaminar and interlaminar damage is extremely important for the structural response of laminated composite structures. This subject has gained particular interest in recent years due to the introduction in the market of spread-tow, ultra-thin carbon-fibre reinforcements with different configurations. In the present paper, an experimental test campaign was carried out to study the structural response of aerospace-grade plain weave spread-tow fabrics (STFs) of different areal weights. The results showed that, in spite of an apparent superior longitudinal tensile strength of the thick STF, the multidirectional thin-STF laminate exhibited an improved tensile unnotched strength over the thick-STF laminate, attributed to its damage suppression capability. However, damage suppression was also responsible for similar tensile notched strengths. In compression, the thin-STF laminate performed substantially better than the thick-STF laminate in both unnotched and notched configurations. Finally, a similar bearing response was obtained in both STF laminates, in spite of a slightly higher resistance of the thin-STF laminate to the propagation of subcritical damage mechanisms.

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Fernandes, Pedro, José Sena-Cruz, José Xavier, Patrícia Silva, Eduardo Pereira, and José Cruz. "Durability of bond in NSM CFRP-concrete systems under different environmental conditions." Composites Part B: Engineering. 138 (2018): 19-34. AbstractWebsite

Abstract This paper addresses the durability of bond between concrete and carbon fibre reinforced polymer (CFRP) strips installed according to the near-surface mounted (NSM) technique (NSM CFRP-concrete systems) under the effects of two main groups of environmental conditions: (i) laboratory-based ageing conditions; (ii) real outdoor ageing conditions. The bond degradation was evaluated by carrying out direct pullout tests on aged specimens that were previously subjected to distinct environmental conditions for different periods of exposure. Moreover, the degradation of the mechanical properties of the involved materials was investigated. The digital image correlation (DIC) method was used to document the evolution of the deformation fields at the surface over the whole region of interest consisting of concrete and epoxy adhesive at the ligament region. This information supported the discussion about the evolution of the bond resistant mechanism developed in \{NSM\} CFRP-concrete specimens during testing, as well as the assessment of the bond quality of the system. In general, the results obtained from the durability tests conducted have shown that the different exposure environments, which may be considered as quite severe, did not result in significant damage on \{NSM\} CFRP-concrete system. The maximum decrease of about 12% on bond strength was obtained for real outdoor environments. Conversely, a maximum increase of 8% on bond strength was obtained on the specimens exposed to the temperature cycles between -15��C and +60��C. \{DIC\} allowed to document the stress transfer mechanisms established between the \{CFRP\} and the concrete substrate, revealing the crack patterns and the influence widths of the \{CFRP\} reinforcement strips, which were shown to be important for avoiding group effect when using multiple parallel strengthening \{CFRP\} strips.

Crespo, J., A. Majano-Majano, J. Xavier, and M. Guaita. "Determination of the resistance-curve in Eucalyptus globulus through double cantilever beam tests." Materials and Structures. 51 (2018): 77. AbstractWebsite

The prediction of the fracture behaviour through reliable and practical criteria in the design of structural timber elements and connections has become of great importance and demands a proper fracture characterization of the material. Eucalyptus globulus Labill is envisioned as a hardwood species with great potential for high performance structural purposes because of its major mechanical and durability properties, being so far mainly used in paper industry. Experimental research on the identification of the resistance curves to derive the critical strain energy release rate in Eucalyptus globulus L. under pure mode I and RL crack propagation system is performed by means of Double Cantilever Beam tests. Three different data reduction schemes are compared: the Modified Experimental Compliance Method; and two approaches of the Compliance Based Beam Method. These methods take into account the non negligible damage mechanisms at the fracture process zone and have the advantage of being based exclusively on the specimen compliance following an equivalent crack concept, for which crack length monitoring during testing is not required. The Compliance Based Beam Method turns out to be the most appropriate data reduction scheme to obtain the critical energy release rate in eucalyptus because of its simplicity. Concerning this, a high average value of 720�J/m2 was obtained confirming Eucalyptus globulus L. as a promising hardwood species for timber structural design.

Kuhn, P., G. Catalanotti, J. Xavier, M. Ploeckl, and H. Koerber. "Determination of the crack resistance curve for intralaminar fiber tensile failure mode in polymer composites under high rate loading." Composite Structures. 204 (2018): 276-287. AbstractWebsite

This paper presents the determination of the crack resistance curve of the unidirectional carbon-epoxy composite material IM7-8552 for intralaminar fiber tensile failure under dynamic loading. The methodology, proposed by Catalanotti et al. (2014) for quasi-static loading conditions, was enhanced to high rate loading in the order of about 60 ?s-1. Dynamic tests were performed using a split-Hopkinson tension bar, while quasi-static reference tests were conducted on a standard electromechanical testing machine. Double-edge notched tension specimens of different sizes were tested to obtain the size effect law, which in combination with the concepts of the energy release rate is used to measure the entire crack resistance curve for the fiber tensile failure mode. Digital image correlation is applied to further verify the validity of the experiments performed at both static and dynamic loading. The data reduction methodology applied in this paper is suitable for intralaminar fiber failure modes without significant delamination. Sufficient proof is given that quasi-static fracture mechanics theory can also be used for the data reduction of the dynamic tests. It is shown, that the intralaminar fracture toughness for fiber tensile failure of UD IM7-8552 increases with increasing rate of loading.

Cidade, Rafael A., Daniel S. V. Castro, Enrique M. Castrodeza, Peter Kuhn, Giuseppe Catalanotti, Jose Xavier, and Pedro P. Camanho. "Determination of mode I dynamic fracture toughness of IM7-8552 composites by digital image correlation and machine learning." Composite Structures. 210 (2019): 707-714. AbstractWebsite

An optical experimental procedure for evaluating the J-Integral from full-field displacement fields under dynamic loading is proposed in this work. The methodology is applied to measure the J-integral in the dynamic compressive loading of fiber-reinforced composites and to calculate the dynamic fracture toughness associated with the propagation of a kink-band. A modified J-Integral that considers inertia effects is calculated over the full-field measurements obtained by digital image correlation, for double edge-notched specimen of IM7-8552 laminates dynamically loaded in a split-Hopkinson pressure bar (SHPB). A sensibility study is conducted to address the influence of the speckle parameters. The results show good agreement with experimental observations obtained by using a different data reduction method, suggesting the existence of a rising R-curve for the studied material under dynamic loading. Furthermore, it was noticed that the inertia effect can be negligible, indicating a state of dynamic equilibrium in which quasi-static approaches may comfortably be used.